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ASTM-D6348 2010

$44.96

D6348-03(2010) Standard Test Method for Determination of Gaseous Compounds by Extractive Direct Interface Fourier Transform Infrared (FTIR) Spectroscopy

Published By Publication Date Number of Pages
ASTM 2010 15
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1.1 This field test method employs an extractive sampling system to direct stationary source effluent to an FTIR spectrometer for the identification and quantification of gaseous compounds. This test method is potentially applicable for the determination of compounds that ( 1 ) have sufficient vapor pressure to be transported to the FTIR spectrometer and ( 2 ) absorb a sufficient amount of infrared radiation to be detected.

1.2 This field test method provides near real time analysis of extracted gas samples from stationary sources. Gas streams with high moisture content may require conditioning to minimize the excessive spectral absorption features imposed by water vapor.

PDF Catalog

PDF Pages PDF Title
1 Scope
2 Referenced Documents
Terminology
4 Summary of Test Method
Significance and Use
Interferences
5 Apparatus
Reagents and Materials
Hazards
6 Reference Spectra
Procedure
7 Calculations ā€“ Data Quantification
Post Test QA/QC
Reporting
Precision and Bias
Keywords
A1. TEST PLAN REQUIREMENTS
A1.1
A1.2
A1.3
A1.4
8 A2. DETERMINATION OF FTIR MEASUREMENT SYSTEM MINIMUM DETECTABLE CONCENTRATIONS (MDC) AND OVERALL CONCENTRATION UNCERTAINTIES
A2.1 Determination of FTIR Measurement System Minimum Detectable Concentration
A2.2 Pre-Test Estimate of Instrument Noise-Limited Minimum Detectable Concentration. MDC#1
A2.3 Pre-Test Estimate of Analytical Algorithm Error Minimum Detectable Concentrations. MDC#2 & MDC#3
FIG. A1.1
9 A2.4 Field Verification of MDCā€”Measurement System Minimum Detectable Concentration
A2.5 Post Test Estimates of Detection Limit
10 A3. FTIR REFERENCE SPECTRA
A3.1
A3.2
A3.3
A3.4
11 A4. REQUIRED PRE-TEST PROCEDURES
A4.1
A4.2
A4.3
A4.4
A4.5
A4.6
A4.7
A4.8
A4.9
12 A5. ANALYTE SPIKING TECHNIQUE
A5.1
A5.2
A5.3
A5.4
A5.5
FIG. A4.1
13 A5.6
A5.7
A5.8
A6. DETERMINATION OF SYSTEM PERFORMANCE PARAMETERSā€”NOISE EQUIVALENT ABSORBANCE (NEA), LINE POSITION, RESOLUTION, AND DETECTOR LINEARITY
A6.1 NEA
A6.2 Line Position
A6.3 Resolution
14 A6.4 Detector Linearity
A7. PREPARATION OF ANALYTICAL QUANTIFICATION ALGORITHM
A7.1
A7.2
A7.3
A7.4
A7.5
A7.6
A8. POST-TEST QUALITY ASSURANCE/QUALITY CONTROL PROCEDURES
A8.1
A8.2
A8.3
A8.4
15 REFERENCES
ASTM-D6348 2010
$44.96