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ASTM-D6508 2005

$44.96

D6508-00(2005)e2 Standard Test Method for Determination of Dissolved Inorganic Anions in Aqueous Matrices Using Capillary Ion Electrophoresis and Chromate Electrolyte

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ASTM 2005 17
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1.1 This test method cover the determination of the inorganic anions fluoride, bromide, chloride, nitrite, nitrate, ortho-phosphate, and sulfate in drinking water, wastewater, and other aqueous matrices using capillary ion electrophoresis (CIE) with indirect UV detection. See Figs. 1-6.

1.2 The test method uses a chromate-based electrolyte and indirect UV detection at 254 nm. It is applicable for the determination or inorganic anions in the range of 0.1 to 50 mg/L except for fluoride whose range is 0.1 to 25 mg/L.

1.3 It is the responsibility of the user to ensure the validity of this test method for other anion concentrations and untested aqueous matrices.

Note 1The highest accepted anion concentration submitted for precision and bias extend the anion concentration range for the following anions: Chloride to 93 mg/L, Sulfate to 90 mg/L, Nitrate to 72 mg/L, and ortho-phosphate to 58 mg/L.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
FIG. 1
FIG. 2
2 Terminology
FIG. 3
FIG. 4
FIG. 5
FIG. 6
3 Summary of Test Method
FIG. 7
FIG. 8
4 Significance and Use
Interferences
Apparatus
FIG. 9
5 Reagents and Materials
FIG. 10
6 Precautions
7 Sampling
Preparation of Apparatus
Calibration
Procedure
Calculation
8 Report Format
Quality Control
Precision and Bias
9 Keywords
TABLE 1
10 TABLE 2
11 TABLE 3
12 TABLE 4
13 TABLE 5
14 TABLE 6
15 A1. Data
A1.1
A1.2 Calibration Linearity
A1.3 Quality Control Solution Preparation
TABLE 7
TABLE A1.1
16 A1.4 Youden Pair Spiking Solution Preparation
A1.5 Sample Matrix Preparation
A1.6 Test Method Detection Limits
TABLE A1.2
TABLE A1.3
TABLE A1.4
TABLE A1.5
17 X1. SUGGESTED BACKGROUND REFERENCES
TABLE A1.6
ASTM-D6508 2005
$44.96