BS EN 10136:2019 – TC:2020 Edition
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Tracked Changes. Steels and cast irons. Determination of nickel content. Flame atomic absorption spectrometric method (FAAS)
| Published By | Publication Date | Number of Pages |
| BSI | 2020 | 39 |
This document specifies a flame atomic absorption spectrometric method (FAAS) for the determination of nickel content in steels and cast irons. The method is applicable to nickel contents between 0,004 % (weight percent) and 2,0 % (weight percent). The method can be adapted to lower or higher nickel contents by changing the test portion or the dilution process, provided the criteria in 6.2.2 and 6.2.3 are still met.
PDF Catalog
| PDF Pages | PDF Title |
|---|---|
| 25 | undefined |
| 29 | 1 Scope 2 Normative references 3 Terms and definitions 4 Principle 5 Reagents |
| 31 | 6 Apparatus 6.1 Ordinary laboratory apparatus 6.2 Atomic absorption spectrometer 6.2.1 General 6.2.2 Minimum precision 6.2.3 Additional performance requirements 6.2.3.1 General 6.2.3.2 Characteristic concentration 6.2.3.3 Limit of detection 7 Sampling |
| 32 | 8 Procedure 8.1 Test portion 8.2 Blank test 8.3 Determination 8.3.1 Preparation of the test solution 8.3.2 Treatment of the test solution 8.3.2.1 Nickel contents up to 0,10 % 8.3.2.2 Nickel contents between 0,08 % and 2,0 % |
| 33 | 8.3.3 Preparation of the calibration solutions 8.3.3.1 General 8.3.3.2 Nickel contents up to 0,10 % 8.3.3.3 Nickel contents between 0,08 % and 2,0 % |
| 34 | 8.3.4 Adjustment of the atomic absorption spectrometer 8.3.5 Spectrometric measurements 8.3.5.1 Spectrometric measurement of the calibration solutions |
| 35 | 8.3.5.2 Spectrometric measurement of the test solutions 9 Expression of results 9.1 Use of the calibration curve 9.2 Use of bracketing method |
| 36 | 10 Test report |
| 37 | Annex A (informative)Precision A.1 General A.2 Repeatability A.3 Reproducibility |
