BS ISO 18144:2003:2009 Edition

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Environmental tobacco smoke. Estimation of its contribution to respirable suspended particles. Method based on solanesol

Published By	Publication Date	Number of Pages
BSI	2009	24

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Categories: 13.040.20 - Ambient atmospheres, BSI

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Description

This International Standard specifies a method for the sampling and determination of respirable suspended particles (RSP) and for the estimation of the RSP fraction attributable to environmental tobacco smoke (ETS). This method is applicable to personal and area sampling. This method is compatible with the determinations of gravimetric RSP, ultraviolet particulate matter (UVPM) and fluorescent particulate matter (FPM), which are also used to estimate the contribution of ETS to RSP.

NOTE See ISO 15593^[3] for details.

PDF Catalog

PDF Pages	PDF Title
3	TitlePage – Environmental tobacco smoke�— Estimation of its contribution to respirable suspended …
5	TableofContent – Contents Page
6	Foreword – Foreword
7	Introduction – Introduction
9	Scope – 1�� Scope NormativeReference – 2�� Normative references
10	Clause1 – 4�� Principle Clause1 – 5�� Limits and detection Clause1 – 6�� Reagents UntitledSubclause2 – 6.1�� Acetonitrile UntitledSubclause2 – 6.2�� Methanol UntitledSubclause2 – 6.3�� Solanesol UntitledSubclause2 – 6.4�� Helium UntitledSubclause2 – 6.5�� Solanesol standard solutions UntitledSubclause3 – 6.5.1�� Primary standard of solanesol UntitledSubclause3 – 6.5.2�� Secondary standard of solanesol UntitledSubclause3 – 6.5.3�� Tertiary standard of solanesol
11	UntitledSubclause3 – 6.5.4�� Working standards of solanesol Clause1 – 7�� Apparatus UntitledSubclause2 – 7.1�� Sample collection system UntitledSubclause3 – 7.1.1�� Polytetrafluoroethylene (PTFE) membrane filter UntitledSubclause3 – 7.1.2�� Filter cassette UntitledSubclause3 – 7.1.3�� Bubble flowmeter UntitledSubclause3 – 7.1.4�� Personal sampling pump UntitledSubclause3 – 7.1.5�� Inertial impactor UntitledSubclause3 – 7.1.6�� Stopcock grease UntitledSubclause2 – 7.2�� Analytical system UntitledSubclause3 – 7.2.1�� High-performance liquid chromatography (HPLC) system UntitledSubclause3 – 7.2.2�� HPLC column UntitledSubclause3 – 7.2.3�� Guard cartridge column UntitledSubclause3 – 7.2.4�� Sample containers UntitledSubclause2 – 7.3�� Dispensing pipettes UntitledSubclause2 – 7.4�� Filter forceps UntitledSubclause2 – 7.5�� Wrist-action shaking device UntitledSubclause2 – 7.6�� One-mark pipettes
12	UntitledSubclause2 – 7.7�� One-mark volumetric flasks Clause1 – 8�� Sampling procedure Subclause2 – 8.1�� Calibration of air pumping system Subclause2 – 8.2�� Sample collection
13	Clause1 – 9�� Analytical procedure Subclause2 – 9.1�� Preparation of samples and blanks Subclause2 – 9.2�� Determination of solanesol Subclause3 – 9.2.1�� Setting up the apparatus
14	Subclause3 – 9.2.2�� Analysis of samples and blanks Subclause3 – 9.2.3�� Constructing the solanesol calibration curve
15	Clause1 – 10�� Expression of results Subclause2 – 10.1�� Calculation of solanesol contents Subclause3 – 10.1.1�� Solanesol content in the test solution Subclause3 – 10.1.2�� Solanesol content in the air
16	Subclause2 – 10.2�� ETS-PM contribution to RSP as estimated by solanesol Subclause3 – 10.2.1�� Calculation of Sol-PM Subclause3 – 10.2.2�� Apportionment of RSP as estimated by Sol-PM Clause1 – 11�� Laboratory performance criteria and quality assurance Clause1 – 12�� Repeatability and reproducibility
17	Clause1 – 13�� Test report
18	AnnexInformative – Laboratory performance criteria: Quality assurance measures Clause1 – A.1�� Standard operating procedures (SOPs) UntitledSubclause2 – A.1.1�� Users should generate SOPs describing and documenting the following… UntitledSubclause2 – A.1.2�� The SOPs should provide specific, step-by-step instructions and sho… UntitledSubclause2 – A.1.3�� Solanesol is typically not detected in sample blanks. Detectable qu… UntitledSubclause2 – A.1.4�� Periodically, wipe clean the surface of the inertial impactor and a… UntitledSubclause2 – A.1.5�� In the event that an initial sample result is above the calibration… Clause1 – A.2�� Calibration of personal sampling pumps UntitledSubclause2 – A.2.1�� Calibrate sampling pumps at the beginning and at the conclusion of … UntitledSubclause2 – A.2.2�� Set the pump flow controller using a bubble flowmeter or mass flowm… Clause1 – A.3�� Method sensitivity, precision and linearity UntitledSubclause2 – A.3.1�� The sensitivity of this method is demonstrated by the detection lim… UntitledSubclause2 – A.3.2�� Determining repeatability and reproducibility ensures method precis… UntitledSubclause2 – A.3.3�� Non-linearity in the calibration curve may occur at concentrations … Clause1 – A.4�� Method modification UntitledSubclause2 – A.4.1�� The sampling period described in this method may be extended beyond
19	UntitledSubclause2 – A.4.2�� The flow rate of air through the filter may be increased up to UntitledSubclause2 – A.4.3�� The test solution resulting from the procedure described herein is … Clause1 – A.5�� Safety UntitledSubclause2 – A.5.1�� If spilling of solvent or any of the reagents occurs, take quick an… UntitledSubclause2 – A.5.2�� When preparing standards, as with handling any chemicals, avoid con…
20	Bibliography – Bibliography

Additional information

Status	Confirmed
Pages	24
Publication Date	2009-03-31
ISBN	978 0 580 53122 4
Standard Number	BS ISO 18144:2003
Title	Environmental tobacco smoke. Estimation of its contribution to respirable suspended particles. Method based on solanesol
Identical National Standard Of	ISO 18144:2003
Descriptors	Gas chromatography, Environment (working), Particle size distribution, Chemical analysis and testing, Tobacco testing, Air pollution, Suspensions (chemical), Extraction methods of analysis, Tobacco, Smoke, Particulate air pollutants, Particulate materials, Sampling methods
Publisher	BSI
Committee	AW/40
ICS Codes	13.040.20 - Ambient atmospheres

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BS ISO 18144:2003:2009 Edition

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