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BS ISO 20579-4:2018

$142.49

Surface chemical analysis. Guidelines to sample handling, preparation and mounting – Reporting information related to the history, preparation, handling and mounting of nano-objects prior to surface analysis

Published By Publication Date Number of Pages
BSI 2018 32
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This document identifies information to be reported in a datasheet, certificate of analysis, report or other publication regarding the handling of nano-objects in preparation for surface chemical analysis. This information is needed to ensure reliability and reproducibility of analyses needed to advance research and technology using these materials, and for obtaining appropriate understanding of potential nano-object environmental and biological impacts. Such information is in addition to other details associated with specimen synthesis, processing history and characterization, and should become part of the data record (sometimes identified as provenance information) regarding the source of the material and changes that have taken place since it was originated.

This document includes informative annexes that summarize challenges associated with nano-objects that highlight the need for increased documentation and reporting in a material data record (Annex A) and provide examples of methods commonly used to extract particles from a solution for surface chemical analysis (Annex B). An example set of relevant sample data is shown in Annex C.

This document does not define the nature of instrumentation or operating procedures needed to ensure that the analytical measurements described have been appropriately conducted.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
10 4 Provenance information to be collected or retained regarding the history, handling, storage and processing of nano-objects prior to submission for surface analysis
4.1 Information record
11 4.2 As-synthesized and as-prepared materials
12 4.3 After testing, exposure, treatment or retrieval
5 Information to be reported related to preparing and mounting of nanomaterials for surface chemical analysis
5.1 General
5.2 Initial form or packaging of sample
5.3 Analysis objective or special requirements
5.4 Description of method used to prepare samples for analysis
13 5.5 Method of mounting sample for analysis (see ISO 20579‑1 and ISO 20579‑2 for examples)
14 Annex A (informative) Needs for enhanced documentation and application of surface chemical analysis methods to assist in identifying and avoiding artefacts and misinterpretations involving research and applications of nano-objects
18 Annex B (informative) Example methods for extraction of nano-objects from solution for surface analysis and issues for dispersion of dry particles
24 Annex C (informative) Example sample data: collected, recorded and reported for Ag nanoparticles provided by BAM
28 Bibliography
BS ISO 20579-4:2018
$142.49